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Excellent fight, I particularly loved the scene where Shiki was nearly about to be eaten by those familiar. Nice to see that we had some revelations about him on this scene.
Also he became really badass and even a little bit arrogant in this chapter. Seeing him teasing Nero by saying that he would die with him was something.
That's nice to see him loosing his nerves, he's really cooler than in his normal state where he looks like the good student.
Also let's that he has some good acrobatic and fighting skills, has he practiced some kind of martial arts?